Locate the source, drive and receiving position for this task
Required inputs are expected total consumption, bulk-addition speed, effective increments near the endpoint, residual drips and signal stabilization time. Confirm liquid contact, pressure and destination along each illustrated section before defining drive and connection responsibilities.
Maintain usable small increments near the endpoint
Working capacity must cover expected total consumption, while the controlled stroke must support increments near the endpoint. The minimum command volume is not a validated minimum effective titration dose. Outlet droplets, reversal backlash and mixing delays also affect the endpoint.
| Condition to compare | Information required | Selection affected |
|---|---|---|
| Bulk addition | Expected consumption and available time | Determine capacity and replenishment arrangements |
| Endpoint increment | Minimum effective increment and the relationship between commanded and received volume | Compare usable stroke rather than microstep count alone |
| Detection wait time | Mixing and signal-stabilization time | Coordinate addition, waiting and endpoint determination |
Compare product options against task requirements
The following candidate options match this page's responsibilities. Compare them against the operating conditions described, then check capacity, materials and interfaces on the product pages. Card images show representative configurations; suitability must still be confirmed at actual operating points and by application results.
| Product category | Corresponding role | Confirm before selection |
|---|---|---|
| EA standard piston pump | Finite-stroke metering | Compare configurations by routine dose, total cycle displacement and wetted materials |
| SM miniature piston pump | Discrete metering in compact installations | Check installation space first, then validate working doses and actual accuracy |
Coordinate coarse addition, fine addition and measurement dwell
Prime and confirm the titrant before bulk addition. Adjust step size and waiting time as the response approaches the target. After changing titrant, refilling or stopping, recheck the first dose and actual concentration, retaining cumulative delivery records.
Action records should link commands, valve or interface states and actual received results. When raw material, container or sample identity changes, reconfirm shared paths and conditions permitting the next step. Completion of drive movement alone does not replace task acceptance.
Check endpoint and cumulative volume using standards
Measure incremental and cumulative volume with the actual liquid, then validate endpoint and repeatability against method-specified standards. Record overshoot, drift and dwell separately. Full-stroke calibration alone does not establish endpoint performance.
| Validation scenario | Measurement or observation | Interpretation and action |
|---|---|---|
| Final increment | Measure post-stop drips and actual small increments | For endpoint shifts, check hanging droplets and excess addition |
| Cumulative consumption | Use suitable standards to assess the complete process | Record volume, blanks and endpoint repeatability together |
Record test medium, configuration, installed path and operating sequence; present routine operating points and boundary results separately. Calculations support design discussions, component documentation checks models, and installed measurements confirm the actual task.
After an abnormality or maintenance, first identify which segment needs recovery
Retained droplets, oversized increments, insufficient mixing or an unstable signal may cause endpoint overshoot. Check results from the affected step before resuming.
Retain current source, container identity, completed actions, valve or interface state and actual receiving information. Use the table to locate the stage that changed before deciding to retry, continue or restart. After recovery, recheck the relevant operating point before returning an uncertain action to the automatic cycle.
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References
View references (5)
- [1]FOREACH — EA Piston Pump Datasheet, capacities, drive options and test conditions
- [2]Metrohm — How to transfer manual titration to autotitration (2026)
- [3]FOREACH — EA-2500-PEEK transmission configurations
- [4]Metrohm — Eco Titrator manual, §6.12: DET, MET and SET parameters
- [5]FOREACH — EAS Easy-to-Degas Piston Pump Datasheet